Ispitivanje novog postupka sinteze Schiff-ove baze u mikroreaktorskom sistemu

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Julijana Tadić Petra Pavlović Marina Mihajlović Dušan Mijin Mića Jovanović

Apstrakt

Organska sinteza u kontinualnim sistemima privlači sve više pažnje kako u naučnim istraživanjima tako i u industriji. U laboratorijskim uslovima kontinualni metod sinteze najčešće podrazumeva upotrebu mikroreaktora. Ključna prednost mikroreaktora u odnosu na klasične šaržne reaktore jeste veliki odnos površine i zapremine, koji omogućava bolji prenos mase i toplote, veći stepen konverzije, skraćeno vreme trajanja reakcije, bezbednu, jednostavnu i preciznu regulaciju procesa. U ovom radu ispitivana je sinteza Schiff-ove baze u kontinualnom mikroreaktorskom sistemu, na sobnoj temperaturi. U cilju ostvarenja što većeg prinosa proizvoda varirane su koncentracije rastvora polaznih reaktanata i vreme zadržavanja u mikroreaktoru. Reakcija je kvalitativno praćena na UV-Vis spektrofotometru. Sintetisani benzilidenanilin okarakterisan je temperaturom topljenja i FT-IR podacima.

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Kako citirati
TADIĆ, Julijana et al. Ispitivanje novog postupka sinteze Schiff-ove baze u mikroreaktorskom sistemu. Zbornik Međunarodnog kongresa o procesnoj industriji – Procesing, [S.l.], v. 31, n. 1, p. 23-26, june 2018. Dostupno na: <https://izdanja.smeits.rs/index.php/ptk/article/view/3437>. Datum pristupa: 10 dec. 2018 doi: https://doi.org/10.24094/ptk.018.31.1.23.
Sekcija
Procesne tehnologije

Reference

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